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Beilstein J. Org. Chem. 2015, 11, 1163–1174, doi:10.3762/bjoc.11.131
Graphical Abstract
Scheme 1: Proposed mechanisms via pathways (I) to (III) for the cathodic hydrodimerization of olefins with el...
Scheme 2: Cathodic reduction of nitroalkene 1 to hydrodimer 2 and oxime 5.
Scheme 3: Preparation of the 1-aryl-2-nitroalkenes 1, 4, 8–15.
Scheme 4: Reduction potentials (Ep,c in Volt) of nitroolefins. Conditions: amalgamated gold wire, v = 0.1 V/s...
Figure 1: (a) CV of 15; v = 0.1 V/s, (b) CV of 15; v = 10 V/s.
Scheme 5: Hydrodimerization of nitroalkene 14 and 15.
Scheme 6: (a) Intramolecular hydrocoupling of dinitrodiene 16 and (b) hydrodimerization of 1-nitrocyclohexene...
Scheme 7: Possible stereoisomers and their mirror images for the hydrodimers 2 and 18–23; R and S are the con...
Figure 2: 1H NMR spectrum of 18b (without aromatic H); below experimental spectrum, above: simulated signals ...